Materials Transactions Online

Materials Transactions, Vol.57 No.12 (2016) pp.1979-1984
© 2016 The Japan Institute of Metals and Materials

Evaluations of Mechanical Properties of Electrodeposited Nickel Film by Using Micro-Testing Method

Takashi Nagoshi1, 2, Tso-Fu Mark Chang2 and Masato Sone2

1Advanced Manufacturing Research Institute, National Institute of Advanced Industrial, Science and Technology, Tsukuba 305-8564, Japan
2Institute of Innovative Research, Tokyo Institute of Technology, Yokohama 226-8503, Japan

Compression and tensile testing of electrodeposited nickel films with micro-sized specimens were reviewed. Preparation of micro-specimens without the tapering was realized by the micro-specimen fabrication method developed in our group. Accurate micro-testing method with precisely-shaped specimens is needed to reveal micro-mechanical properties of electrodeposited metals. The micro-testing on nanocrystalline nickel plated by an electrodeposition method with supercritical carbon dioxide showed remarkably high strength, and the strength increased with a decrease in the specimen size. The results indicated grain boundary mediated deformation of the electrodeposited nanocrystalline nickel.

This Paper was Originally Published in Japanese in J. Japan Inst. Met. Mater. 80 (2016) 7-12.

[doi:10.2320/matertrans.MG201622]

(Received 2016/03/18; Accepted 2016/09/01; Published 2016/11/25)

Keywords: micro-testing, electrodeposition, nanocrystalline nickel

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